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Machinable bioceramic foams prepared by gelcasting method
Šťastný, Přemysl ; Částková, Klára (referee) ; Trunec, Martin (advisor)
Diploma thesis is focused on development of method for preparation individualized bioscaffolds prepared by milling of HA foam prepared by gel casting method and consolidated via epoxy curing reaction. Diploma thesis continues in bachelor thesis Modern processing methods of porous bioceramics. Literature search is filled in the newest knowledge from the field of bioactivity enhancement of scaffolds. Experimental part of diploma thesis described development of system for individualized scaffold manufacturing from HA suspension preparation, preparation of ceramic blocks used as material for machining to final blocks machining. Pressure strength of foam were evaluated, too. Chosen samples were coated with calcium polyphosphate coating for biological response enhancement. Coated samples were given for in-vivo test to partner university in Beijing under the terms of project FP7-NMP-2013-EU-China: "Bioscaffolds"
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Separation of pollutants on photoreactors
Kurťák, Marek ; Šolcová, Olga (referee) ; Svěrák, Tomáš (advisor)
The diploma thesis deals with photocatalytic degradation of organic polutants on water- suspended UV activated anatase particles. The measurements are executed on a pilot plant UV photoreactor and the aim the thesis is to figure out the time course of azo dyes degradation under different photoreactor settings and subsequently infer the effectivity of the photoreactor under different settings. The degree of the aze dyes degradation is evaluated via UV-VIS spectrometry.
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Transparent polycrystalline ceramics at visible and infrared wavelenghts
Veselý, Jan ; Maca, Karel (referee) ; Trunec, Martin (advisor)
his thesis deals with preparation of transparent ceramic sheets made out of sub-µm alumina powder. Green bodies are prepared by ultraviolet (UV) curing of UV curable resin containing ceramic powder followed by debinding of organic parts at elevated temperature. High relative density of green bodies is essential for reduction of shrinkage during subsequent sintering process. Therefore high solids loading dispersions containing > 57 vol% ceramic particles are used. To reach transparent behaviour, porosity within the sheets must be reduced completely. Therefore hot isostatic pressing (HIP) is used as a final operation. Finally, light transmission and hardness measurements are presented. Possibilities of making high resolution microstructures using maskless lithography and some suggestions for use of the UV curing technique for production of complex-shaped 3D structures are briefly mentioned.
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Sealing Diaphragm Walls
Kaderka, Jan ; Boštík, Jiří (referee) ; Svoboda, Petr (advisor)
The topic of this thesis is history, the purpose to carry out diaphragm wall, types of the emplyoed technologies and specific examples of its application in practise. Part of this thesis will concantrate on the parametres of bonding agents and the grouting mixtures.
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Characterization of suspension plasma sprayed coatings deposited using different organic carriers
Dukovský, Daniel ; Toma, Filofteia-Laura (referee) ; Čížek, Jan (advisor)
Cílem této bakalářské práce bylo charakterizovat a porovnat povlaky nanesené plazmovým žárovým nanášením ze suspenze s použitím různých organických nosičů. Teoretická část obsahuje stručný popis běžně používaných metod žárového nanášení a blíže se věnuje technologii hybridního vodou stabilizovaného plazmatu (hořák s touto technologií byl využit pro nanesení povlaků v tomto výzkumu). Druhá polovina teoretické části se zabývá věcným popisem povlaků a metodami nanášení prášku o velikosti částic v řádu nanometrů, kde hraje důležitou roli právě použití suspenze. Experimentální část je zaměřena na vliv použitého solventu v suspenzi na charakteristiky výsledného povlaku. V závěrečné části jsou prezentována a diskutována naměřená data a vyhodnoceny výsledky.
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Advanced ceramics for tissue engineering
Vojtíšek, Jan ; Koplík, Jan (referee) ; Bartoníčková, Eva (advisor)
This bachelor´s thesis deals issues of ceramics materials suitable for tissue engineering. An artificial substitute for human tissue can be divided to several generations. This include inert, bioactive and bioresobable materials. Resorbable substitutions are prepared from materials, which could substitute host tissue, for example hydroxyapatite. HA can be prepared in different ways (dry and wet way). To better application in medicine, ceramics foams prepared by in situ foaming or replication technique are using. Experimental part of this paper deals preparing of hydroxyapatite powder and process optimization. Samples was characterized by IR and Raman spectrometry, XRD analysis and particle size was studied by SEM. Ceramics foams was prepared by in situ foaming from Al2O3, HA and composites (in ratio 50 – 50, 75 – 25, 90 – 10). Porosity was evaluated by stereomicroscope, density and level of sintering was studied by SEM microscopy.
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Influence of nanoparticles on polymer chains in solution.
Bayer, Adam ; Chamradová, Ivana (referee) ; Jančář, Josef (advisor)
High surface area of used nanoparticles and their comparable size with polymer chains, are the most important characteristics of fillers in the preparation of non-Newtonian suspensions. Such structures at different concentrations have major influence on the rheological behavior of polymer solution in solvent. With increasing volume fraction of nanofiller, there is pseudoplastic or dilatant behavior present in the dissolved elastomers. Diploma thesis studies the influence of the concentration of different elastomers (SBR and SEBS copolymers) and nanofiller (hydrophobic nanosilica) in suspension, of rheological properties.
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Particle separation from fluid flow
Fejta, Vojtěch ; Urban, Ondřej (referee) ; Štigler, Jaroslav (advisor)
This bachelor thesis deals with the particle separation from fluid flow. The aim of this thesis is to get acquainted with the already existing methods of separation, to study their principles and to describe devices designed for particle separation. The thesis is divided into two main units, the first explains the individual methods of separation, the second describes the specific particle separators, their advantages and disadvantages. The final part of the thesis is devoted to the design of another approach to separation.
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Study on kinetic stability of suspension with magnetorheological properties
Vlachová, Kristýna ; Kráčalík, Milan (referee) ; Smilek, Jiří (advisor)
Sedimentation in magnetorheological (MR) fluids is undesirable for many technological applications. For this reason, several ways have been proposed to prevent sedimentation instability. This thesis deals specifically with the addition of a suitable additive. The topic was examined based on available literature and according to it was suggested a procedure for the experimental part. Two types of MR liquids with different composition and preparation method were prepared. The first suspensions included a water-in-oil emulsion as a carrier liquid and Span 80 and Tween 80 as additives. For the second MR fluids, the continuous phase was a blend of bearing oils and the suspension was stabilized with organoclay. In both cases, carbonyl iron particles with a diameter of 1,8–2,3 µm were used. The kinetic stability of the prepared MR fluids was monitored and compared using an analytical centrifuge.
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